选择冲洗法在碳纳米管内部填充金属粒子

报道一种直接合成纳米碳管衍生材料的方法.利用纳米碳管的表面张力和毛细管作用,经过注入和选择冲洗法的两步法,制备填充铁、钴和镍的纳米碳管.通过选择合适的注入和洗脱溶液,金属粒子只会填充在纳米管内部.使用扫描电镜和扫描透射电镜研究证实金属粒子仅存在于纳米碳管内部.     

LDV measurement,flow visualization and numerical analysis of flow distribution in a close-coupled catalytic converter

Results from an experimental study of flow distribution in a close-coupled catalytic converter (CCC) are presented. The experiments were carried out with a flow measurement system specially designed for this study under steady and transient flow conditions. A pitot tube was a tool for measuring flow distribution at the exit of the first monolith. The flow distribution of the CCC was also measured by LDV system and flow visualization. Results from numerical analysis are also presented. Experimental results showed that the flow uniformity index decreases as flow Reynolds number increases. In steady flow conditions, the flow through each exhaust pipe made some flow concentrations on a specific region of the CCC inlet. The transient test results showed that the flow through each exhaust pipe in the engine firing order, interacted with each other to ensure that the flow distribution was uniform. The results of numerical analysis were quali-tatively accepted with experimental results. They supported and helped explain the flow in the entry region of CCC.     

有机激光质谱分析法

本文简述了有机物激光解吸分析的发展概况,并分别介绍常用的激光飞行时间质谱仪的原理和结构;有机物激光解吸/电离形成离子的过程;影响分析结果的主要参量和因素以及应用情况,其中包括激光解吸/电离与其它软电离技术如FAB、FD、PD-MS等的对比分析结果,最后着重介绍了近几年来基体帮助激光解吸大分子物质的最新成果以及作者的一些研究成果。     

LD泵浦的全固体绿激光器研究

主要论述了用激光二级管(LD)泵浦、内腔倍频的绿激光器的原理和结构。在激光阈值、斜效率的讨论中指出:当LD的泵浦光束在激光晶体中的尺寸越小,光功率密度越高,激光阈值就越低,转换效率就越高;在放大基波的结构中,激光腔镜对基波的反射度越高,基波的放大倍数就越大,转换效率就越高;重点讨论了内腔倍频激光器中的“绿光问题”,指出造成“绿光问题”是由于模式正交分量之间的和频效应与空间烧孔形成的横向饱和;用Poincare图分析了激光器中出现的混沌行为;对如何克服“绿光问题”,得到稳定激光输出提出了几种方案。针对LD的光形状是一个椭圆光锥,选择了用多组透镜准直、棱镜对扩束的泵浦光传输系统方案;对腔体、激光膜层作了概述,具体提出了用平凹腔结构,并把激光膜层直接做在晶体上,可以减少腔内损耗;对YAG-KTP,YVO₄-KTP组合的绿激光器作了研究。在内腔倍频YAG激光器中观察到的实验现象很好地附合理论结果。在YVO₄-KTP的绿激光器中,比内腔倍频YAG激光器较容易得到YAG-KTP组合绿激光器,最大连续输出功率为14.4mW,阈值15.0mW,光-光斜效率为4.1%.YVO₂-KTP绿激光器:最大连续输出120mW,阈值100mW,光-光斜效率为6.3%.     

超细磷酸钙粒度测定的方法研究

探讨了在用激光粒度分析仪测定超细磷酸钙粒度过程中，不同测试条件对超细磷酸钙粒度测试结果的影响。实验结果表明：当泵速为2200转／分，超声强度为10，超声时间为2min，加0。1g／mL六偏磷酸钠为分散剂时．即为测试超细磷酸钙粒度的最佳分散条件。     

Analytical and experimental characterisation of high-precision flexural pivots subjected to lateral loads

This work addresses the parasitic motion of high-precision rotation mechanisms based on flexural pivots subjected to lateral loads. This case has great importance from the mechanical design point of view, since generally flexural pivots support mechanical elements of considerable weight and their rotation is obtained by loading the pivot with a force instead of a pure couple.

From an analytical point of view, the problem is approached by studying the large deflections of an elastic frame. The equilibrium equations are considered and a solution based on the Newton–Raphson method is proposed. This approach is compared with other theoretical approaches. An experimental assessment performed by using laser interferometric techniques is presented. It is shown that the proposed solution allows the influence of lateral loads to be clearly established and proves to be adequate when the most common cases of limited lateral loads and rotations are considered.     

激光扫描显微镜中的扫描系统

叙述了扫描系统在激光扫描显微镜中的作用,扫描器的位置调整。推导出由于扫描器位置的变化而引起的光程变化,提出了机械设计要求。     

VIRTUAL PROCESSING OF LASER SURFACE HARDENING ON AUTOBODY DIES

A new method of collision-free path plan integrated in virtual processing is developed to improve the efficiency of laser surface hardening on dies. The path plan is based on the premise of no collision and the optimization object is the shortest path. The optimization model of collision-free path is built from traveling salesman problem (TSP). Collision-free path between two machining points is calculated in configuration space (C-Space). Ant colony optimization (ACO) algorithm is applied to TSP of all the machining points to fmd the shortest path, which is simulated in virtual environment set up by IGRIP software. Virtual machining time, no-collision report, etc, are put out after the simulation. An example on autobody die is processed in the virtual platform, the simulation results display that ACO has perfect optimization effect, and the method of virtual processing with integration of collision-free optimal path is practical.     

基于80C196KC的激光雕刻机控制系统研制

文章介绍了基于80C196KC为控制核心的激光雕刻机控制系统的硬件设计,实现了对混合式步进电动机和激光电源的控制.应用页面编程的方法,扩展了512 kB片外数据存储器.研究并提出了采用D/A转换器实现激光功率调节的新方法,从而使机床具有斜坡雕刻功能.采用半步偏差一几何最优化方法编制插补程序,实现了对步进电动机的精确控制,提高了机床加工精度.     

非球面补偿板三维面形检测方法的研究

本文对准直激光束检测非球面方法进行了研究。它不用接触被检件表面,同时也无须处理干涉条纹。测量时只要保证激光细束保持一致的入射方向扫描被检表面,用CCD光电探测器检出面形的斜率变化,而后在扫描范围内积分便能获得面形高度。本文以测量光学系统中用于波面补偿目的的旋转对称镜面为例对测量系统进行分析。该系统不仅可以进行一维测量,通过转台旋转亦可进行二维测量,通过面形重构获得三维的被测体面形。给出了三维面形重构方法,并编制数据处理软件,可以把测量数据处理成高度曲线或三维面形。